| Crude drug latin name
| GARDENIAE FRUCTUS |
| Sample
| |
| NMR type
| 1H-NMR |
| Machine
| JEOL ECA600 |
| Magnetic field (MHz)
| 600.17 MHz |
| Solvent
| CD3OD |
| Mesurement temperature (deg)
| 18.400 |
| Number of excitations (times)
| 16 |
| Sample weight
| |
| spectrum
|  |
| Jcamp file
| geniposidic_acid_PROTON-1.jdx (viewer *for windows) |
| FID file
| geniposidic_acid_PROTON-1.jdf |
| Assignment
|
| Assign
|
Peak(ppm)
|
Integral
|
| 6 |
2.07 |
1.08 |
| 9 |
2.68 |
1.08 |
| 6 |
2.80 |
1.10 |
| 5 |
3.13 |
1.07 |
| 2', 3', 4' ,5' |
3.17-3.36 |
|
| 6' |
3.60 |
1.09 |
| 6' |
3.82 |
1.06 |
| 10 |
4.15 |
1.06 |
| 10 |
4.28 |
1.05 |
| 1' |
4.68 |
1.06 |
| 1 |
5.13 |
1.08 |
| 7 |
5.76 |
1.06 |
| 3 |
7.48 |
1.00 |
|
| Compound name
|
Geniposidic Acid（ゲニポシド酸）
|
| Memo
| リファレンスは溶媒に合わせて測定
assignment reference: Guvenalp, Zuhal; Turkish Journal of Chemistry 2006, V30(4), P515-523 |